Microstructural evolution of AZ91 magnesium alloy during extrusion and heat treatment
(1. School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China;
2. China Aviation Planning and Construction Development Co., Ltd., Beijing 100120, China;
3. School of Materials Science and Engineering, Jiangxi University of Science and Technology,
Ganzhou 341000, China)
2. China Aviation Planning and Construction Development Co., Ltd., Beijing 100120, China;
3. School of Materials Science and Engineering, Jiangxi University of Science and Technology,
Ganzhou 341000, China)
Abstract: Microstructural evolution of AZ91 magnesium alloy was investigated during homogenizing annealing treatment, hot extrusion and ageing treatment, respectively. The results exhibited that both the divorced eutectic β-Mg17Al12 and the precipitated β-Mg17Al12 phases appeared in the as-cast alloy. The β-Mg17Al12 phase dissolved into α-Mg matrix mostly and the structure kept fine after the optimized homogenization treatment at 380 °C for 15 h. Dynamic recrystallization and consequent grain refinement occurred during extrusion. The banded β-Mg17Al12 precipitates paralleled to the extrusion direction were observed after ageing treatment. The banded precipitation should be attributed to the solidification segregation which was elongated during the subsequent extrusion. Furthermore, the effects of temperature, holding time of homogenization and ageing treatment, and extrusion processing parameters on the microstructural evolution of AZ91 alloy were also discussed in details according to the experimental results.
Key words: AZ91 alloy; microstructural evolution; Mg17Al12 phase; heat treatment; extrusion