Effect of annealing treatment on morphologies and gas sensing properties of ZnO nanorods
(College of Materials Science and Engineering, Harbin University of Science and Technology, Harbin 150040, China)
Abstract: The high-temperature stabilization of ZnO nanorods synthesized by hydrothermal treatment was investigated. The structure and morphologies of ZnO nanorods were characterized by XRD and SEM, respectively. The thermal stability of ZnO nanorods was also detected by thermal gravity analyzing. Thermal annealing treatment results indicate that ZnO nanorods are fundamentally stable when annealing temperature is lower than 600 °C. When annealing temperature is beyond 600 °C, the diameters of ZnO nanorods obviously decrease and the aggravating tendency of nanorods between each other also increase. Annealing treatment can greatly influence the gas sensing properties of ZnO nanorods. Comparing with ZnO nanorods without annealing treatment, the gas sensing property of ZnO nanorods to H2 with concentration of 2.5×10-6 can increase from 2.22 to 3.56. ZnO nanorods annealed at 400 °C exhibit optimum gas sesing property to H2 gas.
Key words: ZnO nanorods; annealing treatment; gas sensing property