Phase precipitation behavior and tensile properties of as-cast Ni-based superalloy during heat treatment
(1. Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China;
2. University of Chinese Academy of Sciences, Beijing 100049, China)
2. University of Chinese Academy of Sciences, Beijing 100049, China)
Abstract: The phase precipitation behavior and tensile properties of an as-cast Ni-based alloy, IN617B alloy, after solution heat treatment and long-term aging treatment were investigated. Ti(C,N), M6C and M23C6 are the primary precipitates in as-cast microstructure. After solution heat treatment, most of carbides dissolve into the matrix except a few fine Ti(C,N) within grains. During long-term aging at 700 °C, the phase precipitation behaviors of the alloy are characterized as follows: (1) M23C6 carbides at grain boundaries (GBs) transform from film-like shape to cellular shape and gradually coarsen due to the decrease of the surface energy and element aggregation to GBs; (2) M23C6 carbides within grains have a bar-like morphology with a preferential growth direction [110] and have a cube-on-cube coherent orientation relationship with the matrix γ; (3) γ？ particles inhibit the coarsening of M23C6 within grains by constraining the diffusion of formation elements. Furthermore, the tensile strength of the alloy obviously increases, but the ductility significantly decreases after the aging for 5000 h. The alloy has a relatively stable microstructure which guarantees the excellent tensile properties during long-term aging.
Key words: Ni-based superalloy; phase precipitation; carbide; γ？ phase; tensile properties