Effects of non-isothermal annealing on microstructure and mechanical properties of severely deformed aluminum samples: Modeling and experiment
(Department of Materials Science and Engineering, Sharif University of Technology, Azadi Avenue, Tehran, Iran)
Abstract: In order to investigate the evolution of microstructure and flow stress during non-isothermal annealing, aluminum samples were subjected to strain magnitudes of 1, 2 and 3 by performing 2, 4 and 6 passes of multi-directional forging. Then, the samples were non-isothermally annealed up to 150, 200, 250, 300 and 350 °C. The evolution of dislocation density and flow stress was studied via modeling of deformation and annealing stages. It was found that 2, 4 and 6 passes multi-directionally forged samples show thermal stability up to temperatures of 250, 250 and 300 °C, respectively. Modeling results and experimental data were compared and a reasonable agreement was observed. It was noticed that 2 and 4 passes multi-directionally forged samples annealed non-isothermally up to 350 °C have a lower experimental flow stress in comparison with the flow stress achieved from the model. The underlying reason is that the proposed non-isothermal annealing model is based only on the intragranular dislocation density evolution, which only takes into account recovery and recrystallization phenomena. However, at 350 °C grain growth takes place in addition to recovery and recrystallization, which is the source of discrepancy between the modeling and experimental flow stress.
Key words: severe plastic deformation; multi-directional forging; non-isothermal annealing; dislocation density-based model; microstructure; mechanical properties